Mechanical Properties of N,N,N-trimethylchitosan Chloride Films

نویسندگان

  • Douglas de Britto
  • Sérgio P. Campana-Filho
چکیده

Films of chitosan and N,N,N-trimethylchitosan were cast from aqueous solutions. Chitosan was dissolved in 1% acetic acid while deionized water was the solvent for N,N,N-trimethylchitosan chloride. The resulting films presented different mechanical behaviors as evaluated by DMTA. The film of chitosan exhibited an elastic-type behavior while that of N,N,N-trimethylchitosan was typically viscous. No glass transition temperatures were observed; however, a discrete thermal transition was detected at 25 °C in the case of the N,N,N-trimethylchitosan.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Characterization of TiN, CrN and (Ti, Cr) N Coatings Deposited by Cathodic ARC Evaporation

In this investigation PVD Ti-Cr)N coatings were deposited on hardened and tempered tool steel substrates using reactive arc evaporation. Physical and mechanical properties of coatings such as roughness, thickness, phase composition, hardness and modulus young and coefficient friction were evaluated. Phase compositions were studies by X-ray diffraction method. The surface microstructure and morp...

متن کامل

Eudragit® L100/N-trimethylchitosan chloride microspheres for oral insulin delivery.

Effective oral delivery of protein and peptide drugs remains an active topic in scientific research. In this study, matrix type microspheres were prepared with Eudragit® L100 containing N-trimethylchitosan chloride to improve the permeation of insulin across the intestinal epithelium via the paracellular pathway. Insulin loaded microspheres were initially formulated in accordance with a factori...

متن کامل

Synthesis of Polyaniline/Polyamide composites as membrane and investigation of its properties

Practical applications of conducting polymers such as polyaniline as membranes are particulary limitedbecause of their poor mechanical properties. However by mixing polyaniline with some conventional insulatingpolymers such as nylon and preparation composite films through solvent casting or blending, it seems to be asuitable way in order to increase the mechanical properties of the conducting p...

متن کامل

Structural characteristics and tribological properties of TiAlCr(Si)CN nanocomposite films coated on the SPK 1.2080 tool steel using PVD technique

In the present work, structural characteristics and tribological properties of the Ti-Al-Cr-(Si)-C-N nanocomposite films coated on the SPK 1.2080 tool steel byPVD technique have been investigated. The PVD coating process was carried out using Ti (Si) Al and CrAl cathodes at 150 A current, 40 V bias and (Ar)0.1(CH4)0.45(N2)0.45 gas mixture for 50 min. Evaluations were conducted by OM, FESEM, AFM...

متن کامل

On the Investigation of Sol-Gel TiO2 Nanostructured Films Applied on Windshields Pre-Coated with SiO2 Layer by Dip-Coating Method

TiO2-SiO2 photocatalytic nanostructure film on windshield for self-cleaning purposes was prepared via sol–gel dip-coating method. TiO2 films were prepared on automotive glass pre-coated with a SiO2 layer by a dip-coating method followed by annealing at 500 °C for 30min. The films were characterized using X-ray diffraction XRD and scanning electron microscopy SEM, FE-SEM techniques. The TiO2-SiO...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2005